HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Imidazo[1,2-a]pyridin-5-yl)acetic acid → HCID 59636658, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Imidazo[1,2-a]pyridin-5-yl)acetic acid | HCID 18936841 | — |
| Reactant | 4-bromo-3-(4H-1,2,4-triazol-3-yl)thiophen-2-amine | HCID 59636686 | — |
| Product | HCID 59636658 | HCID 59636658 | — |
Reaction Steps
N-(4-bromo-3-(1H-1,2,4-triazol-5-yl)thiophen-2-yl)-2-(imidazo[1,2-a]pyridin-5-yl)acetamide was synthesized from 2-(imidazo[1,2-a]pyridin-5-yl)acetic acid and 4-bromo-3-(1H-1,2,4-triazol-5-yl)thiophen-2-amine according to protocol A. Retention time (min)=7.958, method [6], MS (ESI) 403.0 (M+H); 1H NMR (300 MHz, CD3OD) δ 8.46 (b s, 1H), 8.35 (d, J=2.2 Hz, 1H), 8.12 (d, J=2.2 Hz, 1H), 8.08-7.96 (m, 2H), 7.58 (d, J=7.2 Hz, 1H), 7.16 (s, 1H), 4.64 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08450363B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-38bc6db7469f4414b164bf2a5fe95e3d |
| Source note | uspto-grants-2013_05 |