2-Chloro-3-nitrothiophene → HCID 68759210, compound

HRID 2098147Notes

Reaction equation

HRID 2098147 reaction equation
C([Sn](CCCC)(CCCC)[C:6]1[O:7][CH:8]=[CH:9][N:10]=1)CCC.Cl[C:20]1[S:21][CH:22]=[CH:23][C:24]=1[N+:25]([O-:27])=[O:26]>>[N+:25]([C:24]1[CH:23]=[CH:22][S:21][C:20]=1[C:6]1[O:7][CH:8]=[CH:9][N:10]=1)([O-:27])=[O:26]

Participants

3

Reactant 2

HCID 2201862-Chloro-3-nitrothiopheneHCID 154861832-(Tri-n-butylstannyl)oxazole

Product 1

HCID 68759210HCID 68759210, compound

Procedure

2-(3-nitrothiophen-2-yl)oxazole was prepared from 2-(tributylstannyl)oxazole (0.94 g, 2.62 mmol) and 2-chloro-3-nitrothiophene (0.429 g, 2.62 mmol) according to protocol E. Retention time (min)=1.794, method [1], MS (ESI) 197.0 (M+H).

Sources & evidence

ORD record
ord-c0a6ec0da0bd4ad9bb595502a23e9794
Source dataset
uspto-grants-2013_05
Patent number
US08450363B2

Reaction notes

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