HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-3-nitrothiophene → HCID 68753372, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-3-nitrothiophene | HCID 220186 | — |
| Reactant | 2-(Tributylstannyl)pyrazine | HCID 2737316 | — |
| Product | HCID 68753372 | HCID 68753372 | — |
Reaction Steps
The title compound was prepared from 2-(tributylstannyl)pyrazine and 2-chloro-3-nitrothiophene using protocol E and was purified by flash chromatograpy (hexane:ethyl acetate). Method [7] Retention time 2.38 min by HPLC (MH+ 208).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08450363B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-62dce89518194bfc802d267870c59791 |
| Source note | uspto-grants-2013_05 |