Butyl Acetate → HCID 131730599, compound

HRID 2098231Notes

Reaction equation

[O-2:1].[Zr+4:2].[O-2].[C:4]([O:7][CH2:8][CH2:9][CH2:10][CH3:11])(=[O:6])[CH3:5]>>[O-2:6].[Zr+4:2].[O-2:1].[C:4]([O:7][CH2:8][CH2:9][CH2:10][CH3:11])(=[O:6])[CH3:5]

Participants

Reactant 2

HCID 31272Butyl Acetate

HCID 6452892Zirconium oxide2×

Product 1

HCID 131730599HCID 131730599, compound

Procedure

P-n-propylbenzoic acid (15 g) and butyl acetate (1000 g) were added to the zirconium oxide dispersion (15% by mass aqueous dispersion, 500 g) prepared in the above (1), and concentrated under reduced pressure to be at most about 1000 g for solvent substitution, and then butyl acetate was added thereto for concentration control thereby giving a zirconium oxide/butyl acetate dispersion (2) having a concentration of 6.7% by mass.

Workup

concentrationconcentrated under reduced pressure
additionbutyl acetate was added
concentrationfor concentration control

Sources & evidence

ORD record: ord-858d139d919e4b81b4882162d468534b
Source dataset: uspto-grants-2013_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08450406B2

Reaction notes

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