HuagongsheHuagongshe Chemistry Print Report · For research reference only
Di(succinimido) carbonate → HCID 87276995, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Di(succinimido) carbonate | HCID 676246 | — |
| Reactant | (9H-Fluoren-9-yl)methyl (4-aminophenyl)carbamate | HCID 11450338 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 87276995 | HCID 87276995 | 99.9% |
Reaction Steps
N,N′-Disuccinimidylcarbonate (16.20 g, 63.26 mmol, 1.1 eq) is added at room temperature to a stirred solution of N-(4-aminophenyl)(fluoren-9-ylmethoxy)carboxamide (20.00 g, 60.53 mmol, 1.0 eq) in CH3CN (1100 mL). After stirring overnight at room temperature, the reaction mixture is filtered to afford 28.50 g of the expected crude product as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08450477B2 |
| Source dataset | uspto-grants-2013_05 |
| ORD ID | ord-5c476fb5c3b2471592aca5f737598cdb |
| Source note | uspto-grants-2013_05 |