4-Heptanamine → HCID 66743940, compound

HRID 2098544Notes

Reaction equation

[Br:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][CH:10]=1)[C:5](Cl)=[O:6].[CH3:11][CH2:12][CH2:13][CH:14]([NH2:18])[CH2:15][CH2:16][CH3:17]>>[Br:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][CH:10]=1)[C:5]([NH:18][CH:14]([CH2:15][CH2:16][CH3:17])[CH2:13][CH2:12][CH3:11])=[O:6]

Participants

Reactant 2

HCID 386654-Heptanamine

HCID 74377Benzoyl chloride, 3-bromo-

Product 1

HCID 66743940HCID 66743940, compound

Procedure

Reaction of 3-bromobenzoyl chloride with heptan-4-amine gave 3-bromo-N-(heptan-4-yl)benzamide as a white solid which was used in the next step without additional purification. Yield (2.43 g, 90%).

Sources & evidence

ORD record: ord-8a436222ece24cce82240c08dcd672c3
Source dataset: uspto-grants-2013_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08450527B2

Reaction notes

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