Water → HCID 59592843, compound

Participants

Reaction Steps

A solution of 161 mg of oxone in 2 mL H2O was added to a mixture of 66 mg of (S)-1-(3-(2-(1H-indazol-4-yl)-4-morpholinothieno[3,2-d]pyrimidin-6-yl)phenylthio)propan-2-ol in 4 mL of methanol. The reaction mixture was stirred for 1 h. The mixture was filtered and the filtrate was evaporated. The product was purified by reverse phase HPLC to yield 3 mg of 138. MS (Q1) 536 (M)+

Provenance & Evidence