HRID2099555

反应详情

EQUATION

反应方程式

HRID 2099555 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of [N(CH3)4]2[PtCl4] or K2[PtCl4] in 5 mL of deionized water is added the cyclohexanecarbonitrile (1:1 equivalent). The reaction mixture is stirred for 10 days. Solid is filtered, and the filtrate is evaporated to dryness. A small amount of acetone is added to the residue, and solid is filtered. The filtrate is lyophilized to give the desired product.

WORKUP

后处理

  1. filtrationSolid is filtered
  2. customthe filtrate is evaporated to dryness
  3. additionA small amount of acetone is added to the residue, and solid
  4. filtrationis filtered