Dipotassium tetrachloroplatinate → HCID 131726519, compound

HRID 2099555Notes

Reaction equation

HRID 2099555 reaction equation
[Cl:1][Pt-2:2](Cl)([Cl:4])[Cl:3].[K+].[K+].[CH:8]1([C:14]#[N:15])[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1>O>[Cl:1][Pt-:2]([Cl:4])[Cl:3].[CH:8]1([C:14]#[N:15])[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1

Participants

4

Reactant 2

HCID 61440Dipotassium tetrachloroplatinateHCID 69834Cyanocyclohexane

Product 1

HCID 131726519HCID 131726519, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

To a solution of [N(CH3)4]2[PtCl4] or K2[PtCl4] in 5 mL of deionized water is added the cyclohexanecarbonitrile (1:1 equivalent). The reaction mixture is stirred for 10 days. Solid is filtered, and the filtrate is evaporated to dryness. A small amount of acetone is added to the residue, and solid is filtered. The filtrate is lyophilized to give the desired product.

Workup

  1. filtrationSolid is filtered
  2. customthe filtrate is evaporated to dryness
  3. additionA small amount of acetone is added to the residue, and solid
  4. filtrationis filtered

Sources & evidence

ORD record
ord-887ebcaa93c54a088deb5fa14d7b670d
Source dataset
uspto-grants-2009_08
Patent number
US07569606B2

Reaction notes

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