Carbon Tetrachloride → HCID 86094276, compound

Participants

Reaction Steps

To the solution of bis(6-bromopyridin-2-yl)methanol (1.07 g, 3.11 mmol) in CCl4 (15 mL) and CH2Cl2(15 mL) was added triphenylphophine (1.14 g, 4.36 mmol) and stirred overnight. The mixture was concentrated and the residue was purified by silica gel chromatography (5-10% EtOAc in hexane) to give 2-bromo-6-[(6-bromopyridin-2-yl)(chloro)methyl]pyridine. LRMS m/z (M+H) Calcd: 362.5, found: 362.8.

Provenance & Evidence