HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86602674, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-(4-Hydroxyphenyl)-2-methoxyethan-1-one | HCID 3015614 | — |
| Reactant | HCID 86602295 | HCID 86602295 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86602674 | HCID 86602674 | — |
Reaction Steps
1.8 g of methanesulfonic acid 3-[2,6-dichloro-4-(3,3-dichloro-allyloxy)-phenoxy]-propyl ester, 1.8 g of potassium carbonate and 1.97 g of 1-(4-hydroxy-phenyl)-2-methoxyethanone are stirred in 30 ml of dimethylformamide at 50° C. for 17 hours. The reaction mixture is poured into water and extracted with ethyl acetate. After concentration of the organic phases and purification over silica gel, 1-(4-{3-[2,6-dichloro-4-(3,3-dichloro-allyloxy)-phenoxy]-propoxy}-phenyl)-2-methoxy-ethanone is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07569727B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-d1f156a5651c4f42bbec5ce8f21b0611 |
| Source note | uspto-grants-2009_08 |