1H-Pyrazol-3-amine, 5-methyl- → HCID 57799785, compound

HRID 2101091Notes

Reaction equation

HRID 2101091 reaction equation
[C:1]([CH2:3][C:4]1[C:13]2[O:12][CH2:11][CH2:10][O:9][C:8]=2[CH:7]=[CH:6][C:5]=1[C:14]([OH:16])=O)#[N:2].[NH2:17][C:18]1[CH:22]=[C:21]([CH3:23])[NH:20][N:19]=1>>[CH3:23][C:21]1[NH:20][N:19]=[C:18]([NH:17][C:1]2[NH:2][C:14](=[O:16])[C:5]3[C:4](=[C:13]4[C:8](=[CH:7][CH:6]=3)[O:9][CH2:10][CH2:11][O:12]4)[CH:3]=2)[CH:22]=1

Participants

3

Reactant 2

HCID 931461H-Pyrazol-3-amine, 5-methyl-HCID 57799628HCID 57799628, compound

Product 1

HCID 57799785HCID 57799785, compound

Procedure

Similar procedure as described in example 2c was used, starting from 5-Cyanomethyl-2,3-dihydro-benzo[1,4]dioxine-6-carboxylic acid and 3-amino-5-methylpyrazole to give 6-(5-Methyl-1H-pyrazol-3-ylamino)-2,3-dihydro-7H-1,4-dioxa-7-aza-phenanthren-8-one. LC-MS: m/e 299 (MH+).

Sources & evidence

ORD record
ord-5c73e6a4044c41ffb719b5a0197ff4f9
Source dataset
uspto-grants-2009_08
Patent number
US07572809B2

Reaction notes

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