Bromine → HCID 57672400, compound

Participants

Reaction Steps

To 10.1 (50 mg, 0.23 mmol) was added Br2 (36 mg, 11.6 μl, 0.23 mmol) in AcOH (1 mL) at room temperature. After 1 hour, the red color disappeared to give a pale orange solution. The solution was concentrated and purified by silica gel chromatography (0 to 50% EtOAc/hexanes) to afford a 27.1 (0.0629 g, 90.8% yield).

Provenance & Evidence