Potassium Carbonate → HCID 57672522, compound

Participants

Reaction Conditions

Reaction Steps

To a flask charged with 27.2 (0.8986 g, 2.30 mmol), tetrakis(triphenylphosphine)palladium (0) (0.265 g, 0.230 mmol), and potassium carbonate (0.635 g, 4.59 mmol) in DMF (10 mL) was added trimethylboroxine (0.959 mL, 6.89 mmol). The resulting mixture was then heated at 100° C. overnight. The reaction was allowed to cool and was then filtered and concentrated. The product was purified by silica gel chromatography (0 to 20% EtOAc/Hexanes) yielding 27.3 (0.46 g, 61% yield).

Provenance & Evidence