HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-5-[5-(chloromethyl)-1,3,4-oxadiazol-2-yl]pyridine → HCID 67406980, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-5-[5-(chloromethyl)-1,3,4-oxadiazol-2-yl]pyridine | HCID 28979365 | — |
| Reactant | 2-cyclopropyl-4-(trifluoromethyl)-1H-indole-5-carbonitrile | HCID 67404472 | — |
| Product | HCID 67406980 | HCID 67406980 | — |
Reaction Steps
Synthesized as described in Example 4 using 2-cyclopropyl-4-(trifluoromethyl)-1H-indole-5-carbonitrile and 3-bromo-5-[5-(chloromethyl)-1,3,4-oxadiazol-2-yl]pyridine: 1H NMR (400 MHz, CDCl3) δ 9.05 (d, J=1.7 Hz, 1H), 8.82 (d, J=1.9 Hz, 1H), 8.39 (m, 1H), 7.69 (d, J=8.5 Hz, 1H), 7.59 (d, J=8.5 Hz, 1H), 6.52 (s, 1H), 5.80 (s, 2H), 2.06 (m, 1H), 1.19 (m, 2H), 0.92 (m, 2H); MS (ES) m/z 488 (M+1, isotope for Br) and 490 (M+1, isotope for Br).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07572820B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-5e282b1f367e4f3fb39d99e7529c1080 |
| Source note | uspto-grants-2009_08 |