Picolinohydrazide → HCID 67403802, compound

HRID 2102015Notes

Reaction equation

HRID 2102015 reaction equation
[Cl:1][C:2]1[C:10]2[N:9]=[C:8]([C:11]([F:14])([F:13])[F:12])[N:7]([CH2:15][C:16]([OH:18])=O)[C:6]=2[CH:5]=[CH:4][C:3]=1[C:19]#[N:20].[N:21]1[CH:26]=[CH:25][CH:24]=[CH:23][C:22]=1[C:27]([NH:29][NH2:30])=O>>[Cl:1][C:2]1[C:10]2[N:9]=[C:8]([C:11]([F:12])([F:13])[F:14])[N:7]([CH2:15][C:16]3[O:18][C:27]([C:22]4[CH:23]=[CH:24][CH:25]=[CH:26][N:21]=4)=[N:29][N:30]=3)[C:6]=2[CH:5]=[CH:4][C:3]=1[C:19]#[N:20]

Participants

3

Reactant 2

HCID 255881PicolinohydrazideHCID 67404984HCID 67404984, compound

Product 1

HCID 67403802HCID 67403802, compound

Procedure

Synthesized as described Example 200C from [4-chloro-5-cyano-2-(trifluoromethyl)-1H-benzimidazol-1-yl]acetic acid and 2-pyridinecarbohydrazide: MS (ESI) m/z 405 (M+1).

Workup

  1. customSynthesized

Sources & evidence

ORD record
ord-2b8631e3974c4f4585aa40ea14fab821
Source dataset
uspto-grants-2009_08
Patent number
US07572820B2

Reaction notes

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