HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Bromoethoxy)-4-fluorobenzene → HCID 57800088, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Bromoethoxy)-4-fluorobenzene | HCID 2064171 | — |
| Reactant | 4-chloro-2-propyl-1H-indole-5-carbonitrile | HCID 67404338 | — |
| Product | HCID 57800088 | HCID 57800088 | — |
Reaction Steps
Synthesized as described in Example 4 from 4-chloro-2-propyl-1H-indole-5-carbonitrile and 1-[(2-bromoethyl)oxy]-4-fluorobenzene: 1H NMR (400 MHz, DMSO-d6) δ 7.89 (s, 1H), 7.80 (d, J=8.7 Hz, 1H), 7.54 (d, J=8.5 Hz, 1H), −7.11-6.97 (m, 2H), 6.83-6.71 (m, 2H), 4.64 (t, 2H), 4.20 (t, 2H), 2.88 (t, 2H), 1.70-1.58 (m, 2H), 0.94 (t, J=7.3 Hz, 3H); MS (ES) m/z 357 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07572820B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-0d60fc0e82294dc79ba976f2f8e11ae6 |
| Source note | uspto-grants-2009_08 |