Water → Ammonium, trimethylbutyl-, hydroxide

HRID 2102250Notes

Reaction equation

HRID 2102250 reaction equation
[I-].[CH3:2][N+:3]([CH3:9])([CH3:8])[CH2:4][CH2:5][CH2:6][CH3:7].[OH2:10]>[Ag-]=O>[OH-:10].[CH3:2][N+:3]([CH3:9])([CH3:8])[CH2:4][CH2:5][CH2:6][CH3:7]

Participants

4

Reactant 2

HCID 962WaterHCID 24398N,N,N-Trimethylbutan-1-aminium iodide

Product 1

HCID 45658Ammonium, trimethylbutyl-, hydroxide

Reagents, catalysts & solvents 1

HCID 178418778HCID 178418778, compoundCatalyst

Procedure

A typical TMBAOH solution was prepared as follows. Trimethylbutylammonium iodide, 1466.3 g, was dissolved in 1948.6 g deionized water in a 5 liter 3-necked round bottom flask equipped with overhead stirring. A 1 wt. % excess of silver(I) oxide, (99%), 712 g, was added and stirred in the dark for 24 hours. The resulting trimethylbutylammonium hydroxide solution was isolated by filtration.

Workup

  1. customA typical TMBAOH solution was prepared
  2. customequipped with overhead stirring

Sources & evidence

ORD record
ord-67ce5afa9c754da7b36540919ab24af2
Source dataset
uspto-grants-2009_08
Patent number
US07575737B1

Reaction notes

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