Tetraethoxysilane → HCID 86643014, compound

HRID 2102251Notes

Reaction equation

HRID 2102251 reaction equation
[OH-].[CH3:2][N+:3]([CH3:9])([CH3:8])[CH2:4][CH2:5][CH2:6][CH3:7].C([O:12][Si:13]([O:20]CC)([O:17]CC)[O:14]CC)C>O>[Si:13]([O-:20])([O-:17])([O-:14])[O-:12].[CH3:2][N+:3]([CH3:9])([CH3:8])[CH2:4][CH2:5][CH2:6][CH3:7].[CH3:2][N+:3]([CH2:4][CH2:5][CH2:6][CH3:7])([CH3:9])[CH3:8].[CH3:2][N+:3]([CH2:4][CH2:5][CH2:6][CH3:7])([CH3:9])[CH3:8].[CH3:2][N+:3]([CH2:4][CH2:5][CH2:6][CH3:7])([CH3:9])[CH3:8]

Participants

4

Reactant 2

HCID 6517TetraethoxysilaneHCID 45658Ammonium, trimethylbutyl-, hydroxide

Product 1

HCID 86643014HCID 86643014, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Trimethylbutylammonium hydroxide, (25.66%), 366.4 g, was diluted with 564.8 g deionized water and to it there were added 500.0 g of tetraethylorthosilicate, (98%) with stirring. After hydrolysis was complete, the solution was placed on a rotary evaporator to remove the alcohol. Elemental analysis showed the solution to contain 7.04 wt % Si.

Workup

  1. customAfter hydrolysis
  2. customthe solution was placed on a rotary evaporator
  3. customto remove the alcohol

Sources & evidence

ORD record
ord-adbc2d4134a04b709c4f39039bc73341
Source dataset
uspto-grants-2009_08
Patent number
US07575737B1

Reaction notes

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