2-Amino-5-Nitrophenol → 3,4-Dihydro-2H-benzo[b][1,4]oxazin-7-amine

HRID 2102949Notes

Reaction equation

HRID 2102949 reaction equation
[O:1]1[CH2:6][CH2:5][NH:4][C:3]2[CH:7]=[C:8](N)[CH:9]=[CH:10][C:2]1=2.[NH2:12]C1C=CC([N+]([O-])=O)=CC=1O>>[O:1]1[CH2:6][CH2:5][NH:4][C:3]2[CH:7]=[CH:8][C:9]([NH2:12])=[CH:10][C:2]1=2

Participants

3

Reactant 2

HCID 49847212-Amino-5-NitrophenolHCID 113441023,4-Dihydro-2H-1,4-benzoxazin-6-amine

Product 1

HCID 114805373,4-Dihydro-2H-benzo[b][1,4]oxazin-7-amine

Procedure

The above was prepared using the same procedure as for 3,4-dihydro-2H-benzo[b][1,4]oxazin-6-amine, except 2-amino-5-nitrophenol was used as starting material.

Workup

  1. customThe above was prepared

Sources & evidence

ORD record
ord-fde9fd1cb05249e98686e1b936acf3c9
Source dataset
uspto-grants-2009_08
Patent number
US07576099B2

Reaction notes

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