HCID 11708700, compound → HCID 69053370, compound

HRID 2103008Notes

Reaction equation

HRID 2103008 reaction equation
[OH:1][CH2:2][C:3]1[C:12]2([CH2:15][CH2:14][CH2:13]2)[O:11][C:10]2[C:5](=[C:6]([CH3:19])[C:7]([OH:18])=[C:8]([CH3:17])[C:9]=2[CH3:16])[CH:4]=1.[H][H]>[Pd]>[OH:1][CH2:2][CH:3]1[C:12]2([CH2:15][CH2:14][CH2:13]2)[O:11][C:10]2[C:5](=[C:6]([CH3:19])[C:7]([OH:18])=[C:8]([CH3:17])[C:9]=2[CH3:16])[CH2:4]1

Participants

4

Reactant 2

HCID 11708700HCID 11708700, compoundHCID 178418361HCID 178418361, compound

Product 1

HCID 69053370HCID 69053370, compound

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

3-(Hydroxymethyl)-5,7,8-trimethyl-3,4-dihydrospiro[chromene-2,1′-cyclobutan]-6-ol was prepared by hydrogenation of 3-(hydroxymethyl)-5,7,8-trimethylspiro[chromene-2,1′-cyclobutan]-6-ol with hydrogen in the presence of Pd/C.

Sources & evidence

ORD record
ord-e41bd02f284f4afabe8dda89227de311
Source dataset
uspto-grants-2009_08
Patent number
US07576094B2

Reaction notes

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