HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-4-[dichloro(4-methylphenyl)methyl]benzene → HCID 22475122, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-4-[dichloro(4-methylphenyl)methyl]benzene | HCID 22475001 | — |
| Reactant | HCID 22475147 | HCID 22475147 | — |
| Product | HCID 22475122 | HCID 22475122 | — |
Reaction Steps
Using 4-chlorophenyl-4-methylphenyl-dichloromethane (57 mg, 0.2 mmol) and 4-[4-(4-fluoro-phenyl)-3,6-dihydro-2H-pyridine-1-sulfonyl]-benzene-1,2-diol (69 mg, 0.2 mmol) as a starting material, the title compound was obtained as an off-white crystalline solid (90 mg, 80%) after taking the residue up in hexane/ethyl acetate (4/1), stirring for 10 minutes, filtering the solid and drying.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576088B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-61067ffee6f545989cc1711e81164473 |
| Source note | uspto-grants-2009_08 |