Ethyl 3,4-Dihydroxybenzoate → HCID 69055812, compound

HRID 2103149Notes

Reaction equation

HRID 2103149 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([C:9]([C:12]2[CH:17]=[C:16]([Cl:18])[CH:15]=[C:14]([Cl:19])[CH:13]=2)(Cl)Cl)[CH:5]=[C:6]([Cl:8])[CH:7]=1.[OH:20][C:21]1[CH:22]=[C:23]([CH:29]=[CH:30][C:31]=1[OH:32])[C:24]([O:26][CH2:27][CH3:28])=[O:25]>>[CH2:27]([O:26][C:24]([C:23]1[CH:29]=[CH:30][C:31]2[O:32][C:9]([C:12]3[CH:17]=[C:16]([Cl:18])[CH:15]=[C:14]([Cl:19])[CH:13]=3)([C:4]3[CH:3]=[C:2]([Cl:1])[CH:7]=[C:6]([Cl:8])[CH:5]=3)[O:20][C:21]=2[CH:22]=1)=[O:25])[CH3:28]

Participants

3

Reactant 2

HCID 77547Ethyl 3,4-DihydroxybenzoateHCID 22475086HCID 22475086, compound

Product 1

HCID 69055812HCID 69055812, compound

Procedure

This compound was prepared from bis-(3,5-dichlorophenyl)dichloromethane and ethyl 3,4-dihydroxybenzoate according to Example 269d; light red solid, m.p.: 89° C.; MS: m/e=484 ([M]+).

Sources & evidence

ORD record
ord-b7b405d07c1f4826b23ccc961cf2bbab
Source dataset
uspto-grants-2009_08
Patent number
US07576088B2

Reaction notes

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