Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2103301Generated: October 30, 2026

Sodium Iodide → HCID 68908797, compound

https://huagongshe.com/reaction/2103301

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium IodideHCID 5238—
ReactantDimethylformamideHCID 6228—
ReactantPotassium CarbonateHCID 11430—
Reactant3-Pentyl-8-azabicyclo[3.2.1]octaneHCID 21989852—
ProductHCID 68908797HCID 68908797—

Reaction Steps

Crude (R,S)-1-(3-chloro-2-methylpropyl)-3,4-dihydro-1H-quinolin-2-one (107LH63) (0.094 g), 3-pentyl-8-azabicyclo[3.2.1]octane (0.027 g, 0.15 mmol), NaI (0.100 g, 0.67 mmol), and K2CO3 (0.075 g, 0.54 mmol) in DMF (1 mL) were reacted and purified according to GP20 to give the title compound (107LH74-c5) (0.023 g). HPLC-MS (ammonium acetate) [M+H]+=383.34.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07576100B2
Source datasetuspto-grants-2009_08
ORD IDord-3f73de855a3f46099f1f75b50b6e8b23
Source noteuspto-grants-2009_08