HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-methylbutane → Isopentyltriphenylphosphonium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-methylbutane | HCID 7891 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Product | Isopentyltriphenylphosphonium bromide | HCID 2759379 | 15.7% |
Reaction Steps
Reaction of 3-methylbutylbromide (6.4 g, 42.0 mmol) with triphenylphosphine (10.0 g, 40.0 mmol) following the procedure of 2c affords the title compound as a white solid (2.6 g). MS (m/e): 335 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576108B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-fc5f126eed884237b6e2df83b398f5ef |
| Source note | uspto-grants-2009_08 |