Triphenylphosphine → HCID 22446842, compound

Participants

Reaction Conditions

Reaction Steps

Dissolve (2-bromo-ethyl)-cyclopentane (15.25 g, 86.1 mmol) which was prepared according to Chem. Pharm. Bull. 1992, 40, 9, 2391-2398 in toluene, add triphenyl-phosphine (22.58 g, 86.1 mmol) and stir at 110° C. for 48 h. Cool the reaction mixture to r.t., concentrate and crystallize the product from diethylether to give 31.47 g product. MS (m/e): 359.0 (M+H).

Provenance & Evidence