2,4-Heptanedione, 6-methyl- → HCID 11668064, compound

HRID 2104144Notes

Reaction equation

HRID 2104144 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([Br:8])=[CH:4][C:3]=1[C:9]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)=O.[CH3:17][CH:18]([CH3:26])[CH2:19][C:20](=[O:25])[CH2:21][C:22](=O)[CH3:23]>>[Br:8][C:5]1[CH:4]=[C:3]2[C:2](=[CH:7][CH:6]=1)[N:1]=[C:22]([CH3:23])[C:21]([C:20](=[O:25])[CH2:19][CH:18]([CH3:26])[CH3:17])=[C:9]2[C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

3

Reactant 2

HCID 763542,4-Heptanedione, 6-methyl-HCID 996772-Amino-5-bromobenzophenone

Product 1

HCID 11668064HCID 11668064, compoundYield 55%

Procedure

The title compound was prepared from (2-Amino-5-bromo-phenyl)-phenyl-methanone [example A16] and 6-methyl-2,4-heptanedione according to the procedure of example 1. Yield: 55%. MS: m/z=381 (M).

Sources & evidence

ORD record
ord-48a160ba4cad426b932e626a8d99e6f5
Source dataset
uspto-grants-2009_08
Patent number
US07576217B2

Reaction notes

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