3,5-Heptanedione, 2,6-dimethyl- → 1-(6-Bromo-2-isopropyl-4-phenyl-quinolin-3-yl)-2-methyl-propan-1-one

Participants

Reaction Steps

The title compound was prepared from (2-Amino-5-bromo-phenyl)-phenyl-methanone [example A16] and 2,6-dimethyl-3,5-heptanedione according to the method of example 1, except that the reaction time was of 96 h and the residue was purified by chromatography on aminated silica gel with heptane/ethyl acetate (85:15). Yield: 46%. MS: m/z=395/397 (M).

Provenance & Evidence