Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,1,1-Trifluoro-2,4-pentanedione → HCID 11509542, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,1,1-Trifluoro-2,4-pentanedione | HCID 73943 | — |
| 반응물 | (2-Amino-5-trifluoromethoxy-phenyl)-phenyl-methanone | HCID 767339 | — |
| 용매 | Ethylacetate heptane | HCID 21899848 | — |
| 생성물 | HCID 11509542 | HCID 11509542 | 63% |
반응 단계
The title compound was prepared from (2-Amino-5-trifluoromethoxy-phenyl)-phenyl-methanone [example A6] and 1,1,1-trifluoro-2,4-pentanedione according to the procedure of example 1, except that the reaction time was of 44 h and heptane/ethyl acetate (10:1) was used. Yield: 63%; MS: m/z=399 (M).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07576217B2 |
| 출처 데이터셋 | uspto-grants-2009_08 |
| ORD ID | ord-665bd1ffe1b9419e9c54b11e6dd3a925 |
| 출처 메모 | uspto-grants-2009_08 |