HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 11494642, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Acetylacetone | HCID 31261 | — |
| Reactant | HCID 67549809 | HCID 67549809 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | HCID 11494642 | HCID 11494642 | 55% |
Reaction Steps
The title compound was prepared from (2-Amino-5-trifluoromethoxy-phenyl)-(3-chloro-phenyl)-methanone [example A7] and acetylacetone according to the procedure of example 1, except that the solvent was isopropanol, and heptane/ethyl acetate (1:2) was used. Yield: 55%; MS: m/z=380 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576217B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-75feaed9252f477cb7e238f1b372a03f |
| Source note | uspto-grants-2009_08 |