HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Dimethylamino)pyrrolidine → HCID 11633287, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Dimethylamino)pyrrolidine | HCID 2758519 | — |
| Reactant | HCID 11710932 | HCID 11710932 | — |
| Solvent | Ethylacetate methanol | HCID 21584119 | — |
| Product | HCID 11633287 | HCID 11633287 | 37% |
Reaction Steps
The title compound was prepared from 1-(6-Bromo-2-methyl-4-phenyl-quinolin-3-yl)-2,2,2-trifluoro-ethanone [example 3] and 3-(dimethylamino)pyrrolidine according to the procedure of example 25, except that the reaction time was of 16 h and that ethyl acetate/methanol (9:1) was used. Yield: 37%; MS: m/z=428 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576217B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-cc19e38989b54674b5797e6736ab2da6 |
| Source note | uspto-grants-2009_08 |