HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 11569890, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | 1,1,1-Trifluoro-2,4-pentanedione | HCID 73943 | — |
| Reactant | HCID 67548485 | HCID 67548485 | — |
| Solvent | Ethylacetate heptane | HCID 21899848 | — |
| Product | HCID 11569890 | HCID 11569890 | 55% |
Reaction Steps
The title compound was prepared from (2-Amino-5-iodo-phenyl)-(4-methanesulfonyl-phenyl)-methanone [example A17] and 1,1,1-trifluoro-2,4-pentanedione according to the procedure of example 1, except that the solvent was isopropanol, the reaction time was of 16 h and heptane/ethyl acetate (1:2) was used. Yield: 55%; MS: m/z=519 (M).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576217B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-2a20864a3b1447a0befb58067cacf290 |
| Source note | uspto-grants-2009_08 |