Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Dimethyl Ether | HCID 8254 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | (Perfluorooctyl)propanoyl chloride | HCID 10864135 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 22061606 | HCID 22061606 | — |
Reaction Steps
Sodium azide (6.0 g) was put in a 250 mL round-bottom flask (2-neck) equipped with a thermometer. H2O (20 mL) was added to dissolve sodium azide. It was cooled on an ice-water bath. A solution of 3-(perfluorooctyl)propionyl chloride (12.9 g) in acetone (25 mL) was added dropwise to keep the temperature below 12° C. The mixture was vigorously stirred for 2 h. Dimethyl ether (100 mL) and water (100 mL) are added, and the mixture was vigorously stirred for 1 min. After the separation of two layers, the aqueous layer was extracted with ether (2×50 mL). The ether layers were combined, and are washed with water (3×100 mL) and brine. After drying over MgSO4, the solvent was removed under vacuum to give a mixture of white solid and liquid (12.0 g) that was immediately used for the next reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07576245B2 |
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| Source dataset | uspto-grants-2009_08 |
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| ORD ID | ord-c57d6cdc6c22450c8d9c0fc5112622f0 |
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| Source note | uspto-grants-2009_08 |
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