Methyl chloroglyoxylate → HCID 22934809, compound

HRID 2104415Notes

Reaction equation

[C:1]([C:3]1[CH:9]=[CH:8][C:6]([NH2:7])=[CH:5][CH:4]=1)#[CH:2].Cl[C:11](=[O:16])[C:12]([O:14][CH3:15])=[O:13]>>[CH3:15][O:14][C:12](=[O:13])[C:11]([NH:7][C:6]1[CH:8]=[CH:9][C:3]([C:1]#[CH:2])=[CH:4][CH:5]=1)=[O:16]

Participants

Reactant 2

HCID 79846Methyl chloroglyoxylate

HCID 37600254-Ethynylaniline

Product 1

HCID 22934809HCID 22934809, compound

Procedure

The method described in Referential Example 242 was performed by use of 4-ethynylaniline and methyl chlorooxoacetate, whereby the title compound was obtained.

Sources & evidence

ORD record: ord-d62a020b38844e42804374ecc8b23857
Source dataset: uspto-grants-2009_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07576135B2

Reaction notes

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