3,4-Dichlorobenzeneboronic acid → [4-(3,4-Dichlorophenyl)-8-(Trifluoromethyl)Quinolin-3-yl](Pyridin-2-yl)Methanone

Participants

Reaction Steps

This compound was prepared using the procedure of Example 1, step 5 using (4-chloro-8-trifluoromethyl-quinolin-3-yl)-pyridin-2-yl-methanone in place of [4-chloro-8-(trifluoromethyl)quinolin-3-yl](phenyl)methanone and 3,4-dichlorophenylboronic acid in place of phenyl boronic acid. MS (ESI) m/z 447/449/451 ([M+H]+); 1H NMR (CDCl3) δ 9.22 (s, 1H), 8.52 (d, J=4.6 Hz, 1H), 8.18 (d, J=7.21 Hz, 1H), 7.96 (d, J=7.83 Hz, 1H), 7.84 (m, 2H), 7.61 (m, 1H), 7.42 (m, 3H), 7.13 (dd, J=8.25 and 1.97 Hz, 1H).

Provenance & Evidence