HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methyl-3-phenyl-1H-1,2,4-triazole → HCID 57803888, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methyl-3-phenyl-1H-1,2,4-triazole | HCID 10877408 | — |
| Reactant | (3-ethylphenyl)(2-methyl-5-phenyl-2H-1,2,4-triazol-3-yl)methanol | HCID 57803786 | — |
| Reactant | 2,4-Difluoro-5-methoxybenzaldehyde | HCID 57803867 | — |
| Product | HCID 57803888 | HCID 57803888 | 74.1% |
Reaction Steps
According to the procedure for Intermediate 370.2, 1-methyl-3-phenyl-1H-1,2,4-triazole (70 mg, 0.44 mmol) and Intermediate 391.1 (80 mg, 0.48 mmol) afforded 108 mg of Intermediate 391.2 as a white solid. LCMS 332.28 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07576098B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-93d4bd16c2cf426cb505b58f83242f38 |
| Source note | uspto-grants-2009_08 |