HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Chloro-4-fluoroanisole → 4-Chloro-2-fluoro-5-methoxybenzaldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Chloro-4-fluoroanisole | HCID 2773580 | — |
| Edukt | 4-Chloro-5-ethyl-2-fluorobenzaldehyde | HCID 57803801 | — |
| Produkt | 4-Chloro-2-fluoro-5-methoxybenzaldehyde | HCID 14928268 | — |
Reaktionsschritte
Following the procedure for Intermediate 390.2, 2-chloro-4-fluoro-1-methoxybenzene (1.0 g, 6.3 mmol) afforded 840 mg of Intermediate 392.1 as a white solid. 1H NMR (400 MHz, CDCl3) δ ppm 3.91 (s, 3H) 6.90-7.00 (m, 1H) 7.41 (dd, J=9.35, 6.32 Hz, 1H) 10.27 (s, 1H)
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07576098B2 |
| Quelldatensatz | uspto-grants-2009_08 |
| ORD ID | ord-cbf9c140bb5848978b2d937d778b9ddc |
| Quellennotiz | uspto-grants-2009_08 |