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HRID2105096

反应详情

EQUATION

反应方程式

HRID 2105096 的结构方程式

REACTANTS

反应物

3
结构：Clc1ccc(Cl)cc1
HCID4685

1,4-Dichlorobenzene

C6H4Cl2

结构：CC1=Nc2ccccc2C1(C)C
HCID15427

2,3,3-Trimethylindolenine

C11H13N

结构：COCCOCCBr
HCID123532

1-Bromo-3,6-dioxaheptane

C5H11BrO2

PRODUCTS

生成物

1
结构：COCCOCC[N+]1=C(C)C(C)(C)c2ccccc21.[Br-]
HCID68813660

未命名化合物

CONDITIONS

反应条件

温度
70 °C

PROCEDURE

实验过程

To 2,3,3-trimethylindolenine (1.59 g) was added 1-bromo-2-(2-methoxyethoxy)ethane (2.75 g) and dichlorobenzene (5 ml). The mixture was heated to 70° C. overnight. The volatiles were stripped and the material purified by HPLC.

WORKUP

后处理

  1. customthe material purified by HPLC