HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dichlorobenzene → HCID 14298267, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dichlorobenzene | HCID 4685 | — |
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Benzothiazole, 2-methyl-6-nitro- | HCID 76250 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 14298267 | HCID 14298267 | — |
Reaction Conditions
| Temperature | 120 °C |
|---|
Reaction Steps
To 2-methyl-6-nitrobenzothiazole (0.36 g) was added ethyl iodide (1.5 ml) and dichlorobenzene (20 ml). The mixture was heated to 120° C. for 2 days and then allowed to cool to room temperature. Ethyl acetate was added and the resulting precipitate removed by filtration. Drying in a vacuum oven gave the desired material (80 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07579140B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-579d121d2d62472e835a9521a51b51f6 |
| Source note | uspto-grants-2009_08 |