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HRID2105103

反应详情

EQUATION

反应方程式

HRID 2105103 的结构方程式

REACTANTS

反应物

2
结构：COCCOCCBr
HCID123532

1-Bromo-3,6-dioxaheptane

C5H11BrO2

结构：CC1=Nc2ccccc2C1(C)CCCCCC(=O)O
HCID57937748

未命名化合物

PRODUCTS

生成物

1
结构：COCCOCC[N+]1=C(C)C(C)(CCCCCC(=O)O)c2ccccc21.[Br-]
HCID68813228

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

CONDITIONS

反应条件

温度
90 °C

PROCEDURE

实验过程

To 6-(2,3-dimethyl-3H-indol-3-yl)hexanoic acid (100 mg) was added 1-bromo-2-(2-methoxyethoxy)ethane (1 ml) and the mixture heated to 90° C. overnight. On cooling diethyl ether (10 ml) was added and the material removed by filtration.

WORKUP

后处理

  1. additionwas added
  2. customthe material removed by filtration