HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 68462725, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Bromomethylcyclopropane | HCID 81503 | — |
| Reactant | HCID 16679702 | HCID 16679702 | — |
| Product | HCID 68462725 | HCID 68462725 | 29% |
Reaction Steps
The title compound was synthesized in analogy to example 17, from 9-(3-pyrrolidin-1-yl-propoxy)-2,3,4,5-tetrahydro-[1,4]diazepino[1,2-a]indol-1-one (example 16), 1-(bromomethyl)cyclopropane and sodium hydride, to give the desired product as a white solid (29%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07579351B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-cdfb56e76c794a05a23af6e841f20e5f |
| Source note | uspto-grants-2009_08 |