Sodium Hydroxide → HCID 86613671, compound

HRID 2105632Notes

Reaction equation

HRID 2105632 reaction equation
[CH2:1]([C@H:7]1[CH2:11][CH:10]([CH3:12])[O:9][C:8]1=[O:13])[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[OH-:14].[Na+:15]>C(O)C>[OH:9][CH:10]([CH3:12])[CH2:11][C@H:7]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH3:6])[C:8]([O-:13])=[O:14].[Na+:15]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 57809406(3S)-3-Hexyl-5-methyloxolan-2-one

Product 1

HCID 86613671HCID 86613671, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Conditions

Temperature
75 °C

Procedure

To an ethanol solution of the compound prepared in Example 1(6) was added an equivalent of an aqueous solution of sodium hydroxide, and the mixture was stirred at 75° C. for 3 hours. The reaction mixture was concentrated to give the compound of the present invention having the following physical data.

Workup

  1. concentrationThe reaction mixture was concentrated
  2. customto give the compound of the present invention

Sources & evidence

ORD record
ord-1516e44be0fa4d68829fa8e60baec042
Source dataset
uspto-grants-2009_08
Patent number
US07579375B2

Reaction notes

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