HuagongsheHuagongshe Chemistry Print Report · For research reference only
Stearoyl chloride → HCID 22182269, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Stearoyl chloride | HCID 8212 | — |
| Reactant | 1-Hydroxy-4-benzoyloxy-2,2,6,6-tetramethylpiperidine | HCID 688178 | — |
| Product | HCID 22182269 | HCID 22182269 | 60% |
Reaction Steps
Using 1-hydroxy-4-benzoyloxy-2,2,6,6-tetramethylpiperidine, prepared as described by Kurumada T. et. al., loc.cit., and stearoyl chloride in a procedure otherwise similar to the preparation of the compound 101 gives a 60% yield of the compound 109 which is obtained in the form of colourless crystals; melting point: 85-89° C. (acetonitrile).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07579411B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-ee42f042d08b41cc886103fd3b04e95b |
| Source note | uspto-grants-2009_08 |