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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2105808Generated: November 1, 2026

Methyl acetoacetate → HCID 58998941, compound

https://huagongshe.com/reaction/2105808

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl acetoacetateHCID 7757—
ReactantCyclohexylamineHCID 7965—
Reactant2-CyclohexylethylamineHCID 20509—
Reactant2-Bromo-1-(5-fluoro-2-methoxyphenyl)ethanoneHCID 2756985—
ProductHCID 58998941HCID 58998941—

Reaction Steps

The title compound was synthesized in analogy to Example 68, using 3-oxo-butyric acid methyl ester as compound of formula R, 2-bromo-1-(5-fluoro-2-methoxy-phenyl)-ethanone as compound of formula S, 2-cyclohexyl-ethylamine as R3—(CH2)m—NH2 and cyclohexylamine as R1R2NH, MS (ISP) 441.6 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07579369B2
Source datasetuspto-grants-2009_08
ORD IDord-3fed8bcee812428d8ee28082791b61a1
Source noteuspto-grants-2009_08