HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Iodobutane → HCID 86086014, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Iodobutane | HCID 10559 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 68813278 | HCID 68813278 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86086014 | HCID 86086014 | — |
Reaction Steps
Preparation according to Example 2: 4-[2-fluoro-3-(trifluoromethyl)phenyl]piperidin-4-ol (0.02 g, 0.076 mmol), acetonitrile (2 ml), potassium carbonate (0.02 g, 0.14 mmol), 2-iodobutane (0.009 ml, 0.082 mmol). MS m/z (relative intensity, 70.eV) 319 (M+, 2), 290 (72), 191 (28), 177 (14), 56 (bp).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07579474B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-69faa04f9ac448cfb3c3f8dd67ebd0ea |
| Source note | uspto-grants-2009_08 |