HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 86616522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1,1,1-Trifluoro-3-iodopropane | HCID 156165 | — |
| Reactant | HCID 68813278 | HCID 68813278 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86616522 | HCID 86616522 | — |
Reaction Steps
Preparation according to Example 2: 4-[2-fluoro-3-(trifluoromethyl)phenyl]piperidin-4-ol (0.02 g, 0.076 mmol), acetonitrile (2 ml), potassium carbonate (0.02 g, 0.14 mmol), 1,1,1-trifluoro-3-iodopropane (0.010 ml, 0.082 mmol). MS m/z (relative intensity, 70 eV) 359 (M+, 20), 276 (bp), 258 (39), 191 (21), 152 (19).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07579474B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-ca1cc296e6e34fee9923f5d144e3cd4c |
| Source note | uspto-grants-2009_08 |