Sodium borohydride → HCID 57810575, compound

Participants

Reaction Steps

A solution of methanesulfonic acid 2-{1-[4-(3,3-dimethyl-2-oxo-butoxy)-3-methyl-phenyl]-1-ethyl-propyl}-benzofuran-6-yl ester (34 mg, 0.069) in THF (5.0 mL) at 0° C. is treated with NaBH4 (13 mg, 0.349 mmol). The resulting mixture is stirred for 30 min at RT and quenched with HCl (1.0 N, 2.0 mL) and extracted with EtOAc (2×10 mL). The organic layer is dried over Na2SO4, concentrated to afford the title compound (30 mg, 88%).

Provenance & Evidence