HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 57810539, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 11329383 | HCID 11329383 | — |
| Product | HCID 57810539 | HCID 57810539 | 74% |
Reaction Steps
[(2-{1-[4-(3,3-Dimethyl-2-oxo-butoxy)-3-methyl-phenyl]-1-ethyl-propyl}-benzofuran-5-carbonyl)-methyl-amino]-acetic acid (Example 9) (47 mg, 0.093 mmol) in THF (2.0 mL) are reacted with NaBH4 (7 mg, 0.18 mmol) analogous to Example 8 to yield title compound (35 mg, 74%). MS (ES) m/e: 508.3 (M−1), 510.3 (M+1)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07579488B2 |
| Source dataset | uspto-grants-2009_08 |
| ORD ID | ord-429b266f286a4dc3b133698acb584481 |
| Source note | uspto-grants-2009_08 |