反应详情

A suspension of 1.30 g (2.83 mmol) ethyl [(1′-benzyl-[1,4′]bipiperidinyl-4-yl)-tert-butoxycarbonyl-amino]-acetate and 0.16 g 10% Pd/C in 25 mL EtOH was hydrogenated for 5 h at 50° C. and 50 psi hydrogen pressure. The catalyst was removed by suction filtering and the filtrate was evaporated to dryness. The product was obtained as a colourless oil, which was reacted further without purification.

1. customThe catalyst was removed by suction
2. filtrationfiltering
3. customthe filtrate was evaporated to dryness
4. customThe product was obtained as a colourless oil, which
5. customwas reacted further without purification