Potassium Hydroxide → HCID 53652481, compound

HRID 2106584Notes

Reaction equation

HRID 2106584 reaction equation
C([O:3][C:4]([CH:6]([O:8][C:9]1[N:13]=[CH:12][N:11]([C:14]2[CH:19]=[CH:18][C:17]([Cl:20])=[CH:16][C:15]=2[Cl:21])[N:10]=1)[CH3:7])=[O:5])C.[OH-].[K+]>C(O)C>[C:4]([CH:6]([O:8][C:9]1[N:13]=[CH:12][N:11]([C:14]2[CH:19]=[CH:18][C:17]([Cl:20])=[CH:16][C:15]=2[Cl:21])[N:10]=1)[CH3:7])([OH:5])=[O:3]

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 14268789HCID 14268789, compound

Product 1

HCID 53652481HCID 53652481, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Seven g of the compound of Example 2 was refluxed for 3 hours with 2.4 g of potassium hydroxide in 100 ml of ethanol, and the product was collected as shown in Example 22 and recrystallized from toluene to obtain 2.3 g of the desired product, m.p. 151°-153°.

Workup

  1. customthe product was collected
  2. customrecrystallized from toluene

Sources & evidence

ORD record
ord-b467bae08bf94e2cbc648cd12be2fc1a
Source dataset
uspto-grants-1990_06
Patent number
US04931083

Reaction notes

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