Potassium Hydroxide → HCID 15016266, compound

HRID 2106589Notes

Reaction equation

HRID 2106589 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([N:9]2[CH:13]=[N:12][C:11]([O:14][CH:15]([C:17]([O:19]CC)=[O:18])[CH3:16])=[N:10]2)[CH:5]=[CH:6][C:7]=1[Cl:8].[OH-].[K+]>C(O)C>[C:17]([CH:15]([O:14][C:11]1[N:12]=[CH:13][N:9]([C:4]2[CH:5]=[CH:6][C:7]([Cl:8])=[C:2]([Cl:1])[CH:3]=2)[N:10]=1)[CH3:16])([OH:19])=[O:18]

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 184262Ethyl 2-{[1-(3,4-dichlorophenyl)-1H-1,2,4-triazol-3-yl]oxy}propanoate

Product 1

HCID 15016266HCID 15016266, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Four g of the compound of Example 6 was refluxed for 4 hours with 1.4 g of potassium hydroxide in 75 ml of ethanol, and the product was collected as shown in Example 22 and recrystallized from ethanol to obtain 3.3 g of the desired product, m.p. 222°-224°.

Workup

  1. customthe product was collected
  2. customrecrystallized from ethanol

Sources & evidence

ORD record
ord-78cd1ea7cce0440e9196e7ce25c09936
Source dataset
uspto-grants-1990_06
Patent number
US04931083

Reaction notes

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